This preliminary program is subject to change.

Advanced On-Line Analytical and Optimization Tools in Pilot Plants


Description:
This session is interested in the application of new on-line analytical technology used in studying reaction kinetics, heat transfer and crystallization in the scale up chemical processes including energetic materials, specialty chemicals, and polymers. The analytical equipment selected to collect kinetics and heat transfer data in pilot plants are very critical in the scale-up of new technologies. Particle size and shape control are often important properties for the application of energetic materials. Gas chromatographs, atomic spectroscopy, and mass spectrometry are also examples of advanced instruments used in pilot plants. With the development of more sophisticated methods to determined these critical properties with greater accuracy scale-up safety is greatly improved.”

Sponsor:
Energetics
Co-Sponsor(s):
Pilot Plants (12b)


Chair:
David C. Attride
Eastman Chemical Company
200 S. Wilcox Dr
Kingsport, TN 37662
Phone Number: 423-229-2692
Email: dattride@eastman.com

Co-Chair:
Shilpa Amato
Branch Manager for Chemical Development
Naval Surface Warfare Center
Indian Head Division
3019 Strauss Ave
Indian Head, MD 20640
Phone Number: 301-744-4273
Fax Number: 301-744-4544
Email: shilpa.amato@navy.mil


Papers:
Optimization and Scale-up of 4,4'-Diamino-3,3'-Azoxyfurazan (DAAF)through the Use of Real-Time Analytical Tools
Kimberly Hanson, Indian Head Division, Naval Surface Warfare Center; Shilpa Amato, Indian Head Division, Naval Surface Warfare Center; Jerry S. Salan, Nalas Engineering Services Inc.; Matt Jorgensen, Nalas Engineering Services Inc.
Energetic Material Process Development Using Scale-Down Experiments
Jerry S. Salan, Nalas Engineering Services Inc.; Matt Jorgensen, Nalas Engineering Services Inc.
Application of in-Situ Technology in 2,6-Diamino-3,5-Dinitropyrazine-1-Oxide (LLM-105) Recrystallizations
Andrew G. Pearsall, Naval Surface Warfare Center; Bradley Sleadd, Naval Surface Warfare Center; Tod F. Ricks, Naval Surface Warfare Center; Shilpa Amato, Indian Head Division, Naval Surface Warfare Center
Taking the Min to the Max: A Case Study in Small Scale Process Development Using On-Line Reaction Calorimetry and in-Situ Particle Characterization
Cheryl Teich, The Dow Chemical Company; Aaron Sarafinas, The Dow Chemical Company; Paul Morton, The Dow Chemical Company
See more of this Group/Topical: Particle Technology Forum