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Tuesday, May 15, 2007 - 2:30 PM

Microstructure Characterization and Property of Plasma Sprayed Nanostructured TBCs

Q. Li, S. Li, W. Yang, Beijing Aeronautical Manufacturing Technology Research Institute, Beijing, China; J. Wu, Wuhan Research Institute of Materials Protection, Wuhan, China

The technology and thermal shock properties and thermal conductivity of plasma sprayed nanostructured yttria-stabilized zirconia thermal barrier coatings are studied in this paper. The TBCs  on  the  substrate of  Ni3Al  based  alloy  IC-10 were fabricated by using of the nanostructured  yttria-stabilized  zirconia  powder under certain plasma  spraying  conditions. By manipulating plasma spray process, the nanostructured TBCs were obtained.  The  specimens  were  thermally  shocked  from   1000°C,  1100 °C  and  1200°C  to  the water which temperature was about 20°C  and  the morphology  and  microstructure of  the  TBCs were  evaluated  by  light  microscopy,  scanning  electron  microscopy (SEM)  and  transmission  electron  microscopy(TEM).  The thermal diffusivity was tested by a laser pulse method. The  results showed that the nanostructured TBCs  had  a  more  than  30%  reduction  in  thermal  conductivity  and the  thermo shock  lifetimes  were  much  longer  than  that  of  the  conventional  TBCs.

Summary: The technology and thermal shock properties and thermal conductivity of plasma sprayed nanostructured yttria-stabilized zirconia thermal barrier coatings are studied in this paper. The TBCs on the substrate of Ni3Al based alloy IC-10 were fabricated by using of the nanostructured yttria-stabilized zirconia powder under certain plasma spraying conditions. By manipulating plasma spray process, the nanostructured TBCs were obtained. The specimens were thermally shocked from 1000�Ž, 1100 �Ž and 1200�Ž to the water which temperature was about 20�Ž and the morphology and microstructure of the TBCs were evaluated by light microscopy, scanning electron microscopy (SEM) and transmission electron microscopy(TEM). The thermal diffusivity was tested by a laser pulse method. The results showed that the nanostructured TBCs had a more than 30% reduction in thermal conductivity and the thermo shock lifetimes were much longer than that of the conventional TBCs.